m-Cyanobenzil

Base Information

• Chemical Name: m-Cyanobenzil
• CAS No.: 56856-42-9
• Molecular Formula: C₁₅H₉NO₂
• Molecular Weight: 235.242
• Mol file: 56856-42-9.mol

Synonyms:m-Cyanobenzil

Chemical Property of m-Cyanobenzil

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of m-Cyanobenzil

There total 4 articles about m-Cyanobenzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

trans-3-cyano stilbene (59089-08-6) → m-Cyanobenzil (56856-42-9)

Guidance literature:

With tert.-butylhydroperoxide; water; tetra-(n-butyl)ammonium iodide; In acetonitrile; at 90 ℃; for 12h;

DOI:10.1021/acscatal.9b05197

Reference yield: 74.0%

3-acethylbenzonitrile (6136-68-1) + benzaldehyde (100-52-7) → m-Cyanobenzil (56856-42-9)

Guidance literature:

With water; dihydrogen peroxide; sodium hydroxide; at 50 ℃; for 10h; Inert atmosphere; Sealed tube; Schlenk technique; Glovebox; Green chemistry;

DOI:10.1039/d0gc03739g

Reference yield:

N-phenyl benzoyl amide (93-98-1,5705-51-1) + 3-Cyanobenzaldehyde (24964-64-5) → m-Cyanobenzil (56856-42-9)

Guidance literature:

N-phenyl benzoyl amide; With thionyl chloride; sodium hydride; In toluene; Reflux;

3-Cyanobenzaldehyde; With sodium hydride; 1,3-dimethylimidazolim iodide; In tetrahydrofuran;

With hydrogenchloride; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2012.02.013

upstream raw materials:

N-phenyl benzoyl amide

3-Cyanobenzaldehyde

trans-3-cyano stilbene

3-acethylbenzonitrile

Downstream raw materials:

C₁₇H₁₄N₄O