4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Base Information

Chemical Name:4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate
CAS No.:1254765-89-3
Molecular Formula:C₂₀H₂₂BNO₇
Molecular Weight:399.208
Hs Code.:

Synonyms:4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Suppliers and Price of 4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

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Technology Process of 4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

There total 4 articles about 4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1254765-89-3
4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1186/s12951-021-00877-6

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 1254765-89-3
4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jacs.8b02279

Reference yield:

: 873-75-6
4-bromobenzenemethanol

: 1254765-89-3
4-nitrophenyl 4-(4’,4’,5’,5’-tetramethyl-1’,3’-dioxa-2’-borolan-2’-yl)benzyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jacs.8b02279