O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

Base Information

Chemical Name:O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate
CAS No.:946076-42-2
Molecular Formula:C₁₈H₂₂ClF₃N₂O₅S₃
Molecular Weight:535.029
Hs Code.:

Synonyms:O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

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Chemical Property of O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

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Technology Process of O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

There total 3 articles about O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 946076-66-0
O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-methoxyimino-5,5,5-trifluoropentyl] dithiocarbonate

: 75-36-5
acetyl chloride

: 946076-42-2
O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2007.04.091

Reference yield:

: 946076-65-9
O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate

: 946076-42-2
O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / ethanol

2: 94 percent / DMAP / CH₂Cl₂ / 2 h / 0 - 20 °C

With pyridine; dmap; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2007.04.091

Reference yield:

: 830-42-2
N-allyl-4-chlorobenzenesulfonamide

: 946076-42-2
O-ethyl S-[1-(N-acetyl-N-(4-chlorobenzenesulfonyl)aminomethyl)-5,5,5-trifluoro-4-methoxyiminopentyl] dithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 74 percent / pyridine / ethanol

3: 94 percent / DMAP / CH₂Cl₂ / 2 h / 0 - 20 °C

With pyridine; dmap; dilauryl peroxide; In ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2007.04.091