Technology Process of C19H20N2O2
There total 4 articles about C19H20N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium hydrogencarbonate; 2-Biphenylcarboxylic acid;
In
1,2-dichloro-ethane;
at 100 ℃;
for 24h;
regioselective reaction;
DOI:10.1021/ol301214u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide / 24 h / 20 °C
2: palladium diacetate; potassium hydrogencarbonate; 2-Biphenylcarboxylic acid / 1,2-dichloro-ethane / 24 h / 100 °C
With
palladium diacetate; benzotriazol-1-ol; potassium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 2-Biphenylcarboxylic acid;
In
water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
2: Fujiwara-Moritani reaction;
DOI:10.1021/ol301214u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide / 24 h / 20 °C
2: palladium diacetate; potassium hydrogencarbonate; 2-Biphenylcarboxylic acid / 1,2-dichloro-ethane / 24 h / 100 °C
With
palladium diacetate; benzotriazol-1-ol; potassium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 2-Biphenylcarboxylic acid;
In
water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
2: Fujiwara-Moritani reaction;
DOI:10.1021/ol301214u