Isobutylidene(ethyl)amine

Base Information

• Chemical Name: Isobutylidene(ethyl)amine
• CAS No.: 1743-56-2
• Molecular Formula: C6H13N
• Molecular Weight: 99.1759
• Hs Code.: 2921199090
• European Community (EC) Number: 217-113-8
• DSSTox Substance ID: DTXSID101299166
• Nikkaji Number: J203.152C
• Mol file: 1743-56-2.mol

Synonyms:Isobutylidene(ethyl)amine;1743-56-2;Ethanamine, N-(2-methylpropylidene)-;N-ethyl-2-methylpropan-1-imine;EINECS 217-113-8;Ethylamine, N-isobutylidene-;(iso-C3H7)CH=NC2H5;N-Ethyl-2-methylpropane-1-imine;N-(2-Methylpropylidene)ethanamine;DTXSID101299166;N-(2-methylpropylidene) ethylamine;AKOS006323320

Chemical Property of Isobutylidene(ethyl)amine

Chemical Property:

• Vapor Pressure: 12.8mmHg at 25°C
• Refractive Index: 1.414
• Boiling Point: 128.7 °C at 760 mmHg
• Flash Point: 22.6 °C
• PSA: 12.36000
• Density: 0.75 g/cm³
• LogP: 1.73310
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 99.104799419
• Heavy Atom Count: 7
• Complexity: 55.2

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN=CC(C)C

Technology Process of Isobutylidene(ethyl)amine

There total 5 articles about Isobutylidene(ethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

N-ethyl-DL-valine nitrile (60726-37-6) → N-isobutylideneethylamine (1743-56-2)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; dicyclohexyl-carbodiimide; at 150 - 160 ℃;

DOI:10.1055/s-1981-29566

Reference yield:

ethylamine (75-04-7,85404-22-4) + isobutyraldehyde (78-84-2) → N-isobutylideneethylamine (1743-56-2)

Guidance literature:

Reference yield:

N,N'-diisobutylideneethane-1,2-diamine (7020-85-1) → 2-isopropyl-1-methyl-1(H)-imidazole (22509-02-0) + N-isobutylidenemethylamine (6898-70-0) + 2,2-dimethylethylenimine (4753-72-4,73311-42-9,218455-16-4) + N-isobutylideneethylamine (1743-56-2) + 1-methyl-2-isopropyl-4,5-dihydroimidazole

Guidance literature:

With lithium iodide; In acetonitrile; for 236h; Product distribution; Irradiation; other diimines, var. Lewis acids, solvents, conc., time;

upstream raw materials:

ethylamine

isobutyraldehyde

N-ethyl-DL-valine nitrile

N,N'-diisobutylideneethane-1,2-diamine

Downstream raw materials:

1-iodo-butane

1-Ethyl-3-isopropyl-2-methyl-2-vinyl-aziridine