N₁-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N₂,2-dimethylalaninamide formate

Base Information

• Chemical Name: N₁-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N₂,2-dimethylalaninamide formate
• CAS No.: 1240516-70-4
• Molecular Formula: CH₂O₂*C₂₅H₂₈ClN₅O₄S₂
• Molecular Weight: 608.139

Synonyms:N₁-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N₂,2-dimethylalaninamide formate

Chemical Property of N₁-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N₂,2-dimethylalaninamide formate

Chemical Property:

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Technology Process of N₁-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N₂,2-dimethylalaninamide formate

There total 1 articles about N₁-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N₂,2-dimethylalaninamide formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

formic acid (64-18-6) + N-[1-{[3-(aminomethyl)phenyl]methyl}-4-methyloxy-1H-indazol-3-yl]-5-chloro-2-thiophenesulfonamide hydrochloride (1240518-04-0) + N-tert-butoxycarbonyl-N-methyl-α-aminoisobutyric acid (146000-39-7) → N1-[(3-{[3-{[(5-Chloro-2-thienyl)sulfonyl]amino}-4-(methyloxy)-1H-indazol-1-yl]methyl}phenyl)methyl]-N2,2-dimethylalaninamide formate (1240516-70-4)

Guidance literature:

N-tert-butoxycarbonyl-N-methyl-α-aminoisobutyric acid; With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In tetrahydrofuran; at 20 ℃;

N-[1-{[3-(aminomethyl)phenyl]methyl}-4-methyloxy-1H-indazol-3-yl]-5-chloro-2-thiophenesulfonamide hydrochloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 2h;

formic acid; In methanol; water; dimethyl sulfoxide; acetonitrile;

upstream raw materials:

formic acid

N-[1-{[3-(aminomethyl)phenyl]methyl}-4-methyloxy-1H-indazol-3-yl]-5-chloro-2-thiophenesulfonamide hydrochloride

N-tert-butoxycarbonyl-N-methyl-α-aminoisobutyric acid

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