6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

Base Information

Chemical Name:6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene
CAS No.:1225352-17-9
Molecular Formula:C₂₁H₂₄BrF₃O
Molecular Weight:429.32
Hs Code.:

Synonyms:6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

Chemical Property:

Boiling Point:458.0±45.0 °C(Predicted)
Density:1.316±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of 6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

There total 6 articles about 6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

: 1225352-13-5
6-bromo-2-(trans-4-tert-butylcyclohexyloxy)-1-iodonaphthalene

: 1225352-17-9
6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;

Reference yield:

: 937-05-3
cis-4-tert-butyl-1-cyclohexanol

: 1225352-17-9
6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 26 h / 0 - 30 °C

3: N-iodo-succinimide / zirconium(IV) chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; N-iodo-succinimide; copper(l) iodide; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; zirconium(IV) chloride; In dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 18508-91-3
methanesulfonic acid 4-tert-butylcyclohexyl ester

: 1225352-17-9
6-bromo-2-(trans-4-tert-butylcvclohexyloxy)-1-(trifluoromethyl)naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 26 h / 0 - 30 °C

2: N-iodo-succinimide / zirconium(IV) chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; N-iodo-succinimide; copper(l) iodide; di-isopropyl azodicarboxylate; triphenylphosphine; zirconium(IV) chloride; In dichloromethane; N,N-dimethyl-formamide; toluene;