9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester
CAS No.:345989-89-1
Molecular Formula:C₄₇H₈₂N₃O₁₃P
Molecular Weight:928.154
Hs Code.:

9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Synonyms:9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

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Chemical Property of 9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

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Technology Process of 9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

There total 3 articles about 9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 178552-55-1
N,N'-(iminodi-2,1-ethanediyl)bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester

: 15205-62-6
tri(tert-butyl)phosphite

: 53229-60-0
4-oxobutanoic acid phenylmethyl ester

: 345989-89-1
9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Guidance literature:: N,N'-(iminodi-2,1-ethanediyl)bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester; 4-oxobutanoic acid phenylmethyl ester; In acetonitrile; at 20 - 80 ℃; for 1h;

tri(tert-butyl)phosphite; In acetonitrile; at 20 ℃; for 96.3333h;
DOI:10.1016/j.tet.2014.05.030

Reference yield:

: 178552-63-1
N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester

: 345989-89-1
9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: platinum on carbon; hydrogen / acetic acid; methanol / 2.5 h / 20 °C

2.1: acetonitrile / 1 h / 20 - 80 °C

2.2: 96.33 h / 20 °C

With platinum on carbon; hydrogen; In methanol; acetic acid; acetonitrile;
DOI:10.1016/j.tet.2014.05.030

Reference yield:

: 146432-43-1
N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester

: 345989-89-1
9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 72 h / 20 °C / Inert atmosphere

2.1: platinum on carbon; hydrogen / acetic acid; methanol / 2.5 h / 20 °C

3.1: acetonitrile / 1 h / 20 - 80 °C

3.2: 96.33 h / 20 °C

With platinum on carbon; hydrogen; potassium carbonate; In methanol; acetic acid; acetonitrile;
DOI:10.1016/j.tet.2014.05.030