N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester

Base Information

• Chemical Name: N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester
• CAS No.: 178552-63-1
• Molecular Formula: C₃₅H₅₉N₃O₈
• Molecular Weight: 649.869

Synonyms:N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester

Chemical Property of N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester

Chemical Property:

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Technology Process of N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester

There total 4 articles about N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester (146432-43-1) + benzylamine (100-46-9) → N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester (178552-63-1)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1016/j.tet.2014.05.030

Reference yield: 37.0%

N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[(methylsulfonyl)oxy]ethyl]glycine 1,1-dimethylethyl ester (871235-17-5) + benzylamine (100-46-9) → N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester (178552-63-1)

Guidance literature:

With potassium carbonate; In acetonitrile; at 45 ℃; for 16h;

DOI:10.1002/ejic.200500018

Reference yield:

2,3-dihydrophthalazine-1,4-dione (1445-69-8) + bromoacetic acid tert-butyl ester (5292-43-3) + N1-(2-aminoethyl)-N1-benzylethane-1,2-diamine (23539-10-8) → N,N'-[[(phenylmethyl)imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]]glycine bis(1,1-dimethylethyl)ester (178552-63-1)

Guidance literature:

With potassium carbonate; In N-methyl-acetamide; hydrazine hydrate;

upstream raw materials:

N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[(methylsulfonyl)oxy]ethyl]glycine 1,1-dimethylethyl ester

benzylamine

2,3-dihydrophthalazine-1,4-dione

bromoacetic acid tert-butyl ester

Downstream raw materials:

9-[1-[bis(1,1-dimethylethoxy)phosphinyl]-4-oxo-4-(phenylmethoxy)butyl]-6,12-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

N'-benzyldiethylenetriamine-N,N,N'',N''-tetraacetic acid

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