(-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

Base Information

Chemical Name:(-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe
CAS No.:186703-39-9
Molecular Formula:C₃₇H₄₃O₇P
Molecular Weight:630.718
Hs Code.:

Synonyms:(-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

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Chemical Property of (-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

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Technology Process of (-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

There total 12 articles about (-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 186703-38-8
(-)-(1S,2R,4S,6R)-1-(Diphenoxyphosphoryloxy)-2,4-bis(benzyloxy)-6-propyloxycyclohexe

: 100-51-6,185532-71-2
benzyl alcohol

: 186703-39-9
(-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1039/a909292g

Reference yield: 60.0%

: 20194-18-7
sodium phenyl-methanolate

: 186703-38-8
(-)-(1S,2R,4S,6R)-1-(Diphenoxyphosphoryloxy)-2,4-bis(benzyloxy)-6-propyloxycyclohexe

: 186703-39-9
(-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/S0040-4039(96)02229-0

Reference yield:

: 100-39-0
benzyl bromide

: 186703-39-9
(-)-(1S,2R,4S,6R)-1-[Bis(benzyloxy)phosphoryloxy]-2,4-bis(benzyloxy)-6-propyloxycyclohexe

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / KH / tetrahydrofuran

2: 65 percent / borontrifluoride etherate

3: 95 percent / TEA, DMAP / CH₂Cl₂

4: 60 percent / tetrahydrofuran

With dmap; TEA; boron trifluoride diethyl etherate; potassium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(96)02229-0