N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

Base Information

Chemical Name:N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide
CAS No.:1234835-71-2
Molecular Formula:C₂₀H₂₃NO₂S
Molecular Weight:341.474
Hs Code.:

Synonyms:N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

Suppliers and Price of N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

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Technology Process of N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

There total 4 articles about N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5162-44-7
1-bromo-4-butene

: 58567-50-3
N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

: 1234835-71-2
N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

Guidance literature:: With potassium carbonate; In acetonitrile; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201503298

Reference yield: 86.0%

: 3360-54-1
3-bromo-2-phenylprop-1-ene

: 10285-80-0
N-tosyl-3-butenylamine

: 1234835-71-2
N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

Guidance literature:: With potassium carbonate; In acetonitrile; Inert atmosphere; Reflux;
DOI:10.1021/ja103901e

Reference yield:

: 5155-87-3
3-phenylbut-3-enoic acid

: 1234835-71-2
N-but-3-en-1-yl-N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: iodine / 1-methyl-pyrrolidin-2-one / 2 h / 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 12 h / Inert atmosphere; Reflux

With iodine; potassium carbonate; In 1-methyl-pyrrolidin-2-one; acetonitrile;
DOI:10.1002/chem.201503298