2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

Base Information

Chemical Name:2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid
CAS No.:1160964-91-9
Molecular Formula:C₁₁H₉F₄NO₄
Molecular Weight:295.19
Hs Code.:

Synonyms:2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

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Chemical Property of 2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

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Technology Process of 2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

There total 1 articles about 2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 374-35-6
3,3,3-trifluoro-2-hydroxy-2-methylpropionic acid

: 446-31-1
2-fluoro-4-aminobenzoic acid

: 1160964-91-9
2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

Guidance literature:: 3,3,3-trifluoro-2-hydroxy-2-methylpropionic acid; With thionyl chloride; In N,N-dimethyl acetamide; at -20 ℃; for 1h;

2-fluoro-4-aminobenzoic acid; In N,N-dimethyl acetamide; at 20 ℃; for 5h;

Reference yield: 82.0%

: 64-17-5
ethanol

: 1160964-91-9
2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

: 1160964-89-5
ethyl 2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoate

Guidance literature:: With sulfuric acid; for 5h; Heating / reflux;

Reference yield: 62.0%

: 1160964-91-9
2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid

: 107-21-1
ethylene glycol

: 1160964-97-5
2-hydroxyethyl 2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]-benzoate

Guidance literature:: 2-fluoro-4-[(3,3,3-trifluoro-2-hydroxy-2-methylpropanoyl)amino]benzoic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 65 ℃; for 2h;

ethylene glycol; In tetrahydrofuran; at 20 - 65 ℃;