meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Base Information

Chemical Name:meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin
CAS No.:139870-31-8
Molecular Formula:C₇₀H₆₈N₁₀O₆
Molecular Weight:1145.37
Hs Code.:

Synonyms:meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

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Chemical Property of meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

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Technology Process of meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

There total 6 articles about meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 535-87-5
3.5-diaminobenzoic acid

: 139870-31-8
meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine / diethyl ether / 1 h / 0 °C

2: thionyl chloride, dimethylformamide / CH₂Cl₂ / 24 h

3: pyridine / CH₂Cl₂; dimethylformamide / 1 h

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 7743-39-7
3,5-bis(acetamido)benzoic acid

: 139870-31-8
meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride, dimethylformamide / CH₂Cl₂ / 24 h

2: pyridine / CH₂Cl₂; dimethylformamide / 1 h

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 139870-31-8
meso-mono<α-o-(3,5-diacetamidobenzenecarboxamido)phenyl>tris(α,α,α-o-pivalamidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / CH₂Cl₂ / 3 h / 0 °C

2: Cl₃CCOOH / CH₂Cl₂ / 0 °C

3: pyridine / CH₂Cl₂; dimethylformamide / 1 h

With pyridine; potassium carbonate; trichloroacetic acid; In dichloromethane; N,N-dimethyl-formamide;