TaCl₂(N(CH₃)2)3(HN(CH₃)2)

Base Information

• Chemical Name: TaCl₂(N(CH₃)2)3(HN(CH₃)2)
• CAS No.: 77071-71-7
• Molecular Formula: C₈H₂₅Cl₂N₄Ta
• Molecular Weight: 429.167
• Mol file: 77071-71-7.mol

Synonyms:TaCl₂(N(CH₃)2)3(HN(CH₃)2)

Chemical Property of TaCl₂(N(CH₃)2)3(HN(CH₃)2)

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of TaCl₂(N(CH₃)2)3(HN(CH₃)2)

There total 1 articles about TaCl₂(N(CH₃)2)3(HN(CH₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

tantalum pentachloride (7721-01-9) + dimethyl amine (124-40-3) → mer,cis-[TaCl3(NMe2)2(NHMe2)] (77071-69-3) + TaCl2(N(CH3)2)3(HN(CH3)2) (77071-71-7) + (TaCl2(N(CH3)2)2(HN(CH3)2))2O (77071-70-6) + N,N-dimethylammonium chloride (506-59-2)

Guidance literature:

In benzene; dimethylamine added to frozen soln.TaCl5 in benzene at -178°C and slowly allowed to warm to room temp. and soln. stirred for 24 h under N2 atm.; Me2NH2Cl filtered, filtrate concd., pentane added slowly, crystals Ta(NMe2)2Cl3(HNMe2) filtered, filtrate allowed to stand for 10 days - Ta(NMe2)3Cl2(HNMe2) and (TaCl2(NMe2)2(HNMe2))2O; elem. anal.;

DOI:10.1021/ic50220a049

upstream raw materials:

tantalum pentachloride

dimethyl amine