4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

Base Information

Chemical Name:4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane
CAS No.:118075-00-6
Molecular Formula:C₃₂H₅₀N₄O₈S₂
Molecular Weight:682.903
Hs Code.:

Synonyms:4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

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Chemical Property of 4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

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Technology Process of 4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

There total 3 articles about 4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 31255-10-4
1,2-bis-(2-bromo-ethoxy)-ethane

: 118074-98-9
4,10-bis<2-(p-tolylsulphonylamino)ethyl>-1,7-dioxa-4,10-diazacyclododecane

: 118075-00-6
4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; Heating;

Reference yield:

: 294-92-8
diaza[12]crown-4

: 118075-00-6
4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / acetonitrile / Heating

2: 73 percent / 45percent aq. NaOH, tetrabutylammonium iodide / Heating

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In acetonitrile;

Reference yield:

: 52601-77-1
4,10-bis(p-tolylsulphonyl)-1,7-dioxa-4,10-diazacyclododecane

: 118075-00-6
4,13-bis(p-tolylsulphonyl)-7,10,19,24-tetraoxa-1,4,13,16-tetra-azabicyclo<14.5.5>hexacosane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / LiAlH₄ / tetrahydrofuran / 20 h / Heating

2: 92 percent / acetonitrile / 1 h / Heating

3: 73 percent / Bu₄NI, 50 percent aq. NaOH / toluene / 16 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; toluene; acetonitrile;