YIIKGVFWDPAC-OCH₃

Base Information

• Chemical Name: YIIKGVFWDPAC-OCH₃
• CAS No.: 131509-64-3
• Molecular Formula: C₇₀H₁₀₀N₁₄O₁₆S
• Molecular Weight: 1425.71

Synonyms:YIIKGVFWDPAC-OCH₃

Chemical Property of YIIKGVFWDPAC-OCH₃

Chemical Property:

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Technology Process of YIIKGVFWDPAC-OCH₃

There total 5 articles about YIIKGVFWDPAC-OCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + Fmoc-Val-OH (68858-20-8) + N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine (35661-39-3,136132-75-7) + Fmoc-Pro-OH (71989-31-6) + N-Fmoc L-Phe (35661-40-6) + Fmoc-(tBu)Asp-OH (71989-14-5) + Fmoc-Ile-OH (71989-23-6,251316-98-0) + Fmoc-Tyr(tBu)-OH (71989-38-3,118488-18-9,204384-67-8) + tert-butyl (S)-5-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-oxohexyl-carbamate (146803-44-3) + 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-mercaptopropionic acid methyl ester (233266-69-8) + 3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester (143824-78-6,163619-04-3) → YIIKGVFWDPAC-OCH3 (131509-64-3)

Guidance literature:

2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-mercaptopropionic acid methyl ester; With N-ethyl-N,N-diisopropylamine; In dichloromethane; trityl chloride resin

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); at 25 ℃; trityl chloride resin Automated synthesizer;

N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Val-OH; Fmoc-Pro-OH; N-Fmoc L-Phe; Fmoc-(tBu)Asp-OH; Fmoc-Ile-OH; Fmoc-Tyr(tBu)-OH; tert-butyl (S)-5-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-oxohexyl-carbamate; 3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester; Further stages;

DOI:10.1021/ol302592v

Reference yield: 41.0%

L-Cysteine methyl ester (2485-62-3) + C82H110N17O19Pol → YIIKGVFWDPAC-OCH3 (131509-64-3)

Guidance literature:

L-Cysteine methyl ester; C₈₂H₁₁₀N₁₇O₁₉Pol; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 4h; not specified

With chlorotriisopropylsilane; water; trifluoroacetic acid;

With tributylphosphine; In tetrahydrofuran; water;

Reference yield:

C112H154N14O22S → YIIKGVFWDPAC-OCH3 (131509-64-3)

Guidance literature:

With 2-ethyl-5-phenylisoxazolium-3'-sulphonate; for 0.5h;

DOI:10.1016/j.bmc.2010.11.006

upstream raw materials:

N-(fluoren-9-ylmethoxycarbonyl)glycine

Fmoc-Val-OH

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

Fmoc-Pro-OH

Downstream raw materials:

YIIKGVFWDPAC(BC₁₀)-OCH₃

YIIKGVFWDPAC(BC₅)-OCH₃

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