Methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate

Base Information

Chemical Name:Methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate
CAS No.:74002-72-5
Molecular Formula:C₈H₁₂O₄
Molecular Weight:172.181
Hs Code.:
NSC Number:252856
DSSTox Substance ID:DTXSID90312346

Synonyms:74002-72-5;NSC 252856;methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate;NSC252856;DTXSID90312346;NSC-252856

Suppliers and Price of Methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate

Chemical Property:

Vapor Pressure:0.01mmHg at 25°C
Boiling Point:263.9°C at 760 mmHg
Flash Point:130.4°C
Density:1.13g/cm³
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:172.07355886
Heavy Atom Count:12
Complexity:223

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC(C(=O)O1)(C)C(=O)OC

Technology Process of Methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate

There total 4 articles about Methyl 3,5-dimethyl-2-oxooxolane-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.8%

: 74002-71-4
methyl 5-methyl-2-oxo-tetrahydrofuran-3-carboxylate

: 74-88-4
methyl iodide

: 74002-72-5
α-methoxycarbonyl-α-methyl-γ-valerolactone

Guidance literature:: With sodium hydride; In benzene; 1.) 80 deg C, 5 h, 2.) r.t., overnight;

Reference yield:

: 123507-71-1
dimethyl (2-methyl-2-propenyl)propanedioate

: 1138334-91-4
C₈H₁₁⁽²⁾HO₄

: C₈H₁₀⁽²⁾H₂O₄

: 74002-72-5
α-methoxycarbonyl-α-methyl-γ-valerolactone

Guidance literature:: With DOTf; In chloroform-d1; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.200800970

Reference yield:

: 108-29-2
5-methyl-dihydro-furan-2-one

: 74002-72-5
α-methoxycarbonyl-α-methyl-γ-valerolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 79.1 percent / NaH / benzene / 3 h / Heating

2: 84.8 percent / NaH / benzene / 1.) 80 deg C, 5 h, 2.) r.t., overnight

With sodium hydride; In benzene;