(2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

Base Information

Chemical Name:(2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅
CAS No.:43017-58-9
Molecular Formula:C₂₄H₂₈BN
Molecular Weight:341.304
Hs Code.:

(2,4,6-(CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>)2BNHC<sub>6</sub>H<sub>5</sub>

Synonyms:(2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

Suppliers and Price of (2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

There total 2 articles about (2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 436-59-9
dimesitylfluoroborane

: 43017-58-9
(2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

Guidance literature:: With C₆H₅NH₂; C₄H₉Li; In diethyl ether; hexane; 30 min stirring;
DOI:10.1016/S0022-328X(00)84991-8

Reference yield:

: 82945-06-0
bis(dimesitylboryl)methane

: 43017-58-9
(2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

: 74178-56-6
methyl(dimesityl)borane

Guidance literature:: With aniline; In tetrahydrofuran; slight excess of C6H5NH2, stirred overnight, solvent was removed under high vac.; detected by (1)H NMR;

Reference yield: 65.0%

: NiBr₂*5/3(THF)

: 43017-58-9
(2,4,6-(CH₃)3C₆H₂)2BNHC₆H₅

: {Ni(N(phenyl)B(2,4,6-trimethylphenyl)2)2}

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; dropwise addn. of BuLi in hexane to HNPhBMes2 in Et2O at 0°C, stirring 30 min., dropwise addn. to NiCl2.5/3(THF)2 in Et2O, stirring 2 h at room temp. (N2); evapn., extn. (hexane), filtration, evapn., cooling to -20°C overnight, crystn.;