benzyl piperazine-1-carbodithioate

Base Information

Chemical Name:benzyl piperazine-1-carbodithioate
CAS No.:91559-28-3
Molecular Formula:C₁₂H₁₆N₂S₂
Molecular Weight:252.404
Hs Code.:

Synonyms:benzyl piperazine-1-carbodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl piperazine-1-carbodithioate

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Technology Process of benzyl piperazine-1-carbodithioate

There total 7 articles about benzyl piperazine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1605349-59-4
tert-butyl 4-(benzylthiocarbonothioyl)piperazine-1-carboxylate

: 91559-28-3
benzyl piperazine-1-carbodithioate

Guidance literature:: tert-butyl 4-(benzylthiocarbonothioyl)piperazine-1-carboxylate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 4h;
DOI:10.1016/j.bmcl.2014.12.062

Reference yield: 67.0%

: 99-00-3
piperazine-1-carbodithioic acid

: 100-39-0
benzyl bromide

: 91559-28-3
benzyl piperazine-1-carbodithioate

Guidance literature:: With sodium hydroxide; In methanol; water;

Reference yield: 54.5%

: 1605349-59-4
tert-butyl 4-(benzylthiocarbonothioyl)piperazine-1-carboxylate

: 91559-28-3
benzyl piperazine-1-carbodithioate

: 109400-03-5
benzyl 4-benzylpiperazine-1-carbodithioate

Guidance literature:: tert-butyl 4-(benzylthiocarbonothioyl)piperazine-1-carboxylate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 6h;

With sodium hydrogencarbonate; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1039/c4ob00005f