4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

Base Information

Chemical Name:4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole
CAS No.:1449115-37-0
Molecular Formula:C₂₁H₃₁N₃O₃SSi
Molecular Weight:433.647
Hs Code.:

Synonyms:4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

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Chemical Property of 4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

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Technology Process of 4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

There total 2 articles about 4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 941-55-9
4-toluenesulfonyl azide

: 1449115-47-2
tert-butyl((4-ethynylcyclohex-3-en-1-yl)oxy)dimethylsilane

: 1449115-37-0
4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

Guidance literature:: With copper(I) thiophene-2-carboxylate; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja405043g

Reference yield:

: 865869-24-5
trifluoro-methanesulfonic acid 4-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enyl ester

: 1449115-37-0
4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: cobalt(III) acetylacetonate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: copper(I) thiophene-2-carboxylate / toluene / 20 °C / Inert atmosphere

With copper(I) thiophene-2-carboxylate; cobalt(III) acetylacetonate; In tetrahydrofuran; toluene;
DOI:10.1021/ja405043g

Reference yield: 86.0%

: 1449115-37-0
4-(4-((tert-butyldimethylsilyl)oxy)cyclohex-1-en-1-yl)-1-tosyl-1H-1,2,3-triazole

: 1449115-07-4
6-((tert-butyldimethylsilyl)oxy)-1-tosyl-4,5,6,7-tetrahydro-1H-indole

Guidance literature:: With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; In 1,2-dichloro-ethane; at 60 ℃; for 4h; Inert atmosphere; Sealed tube;
DOI:10.1021/ja405043g