ethyl styryldiazoacetate

Base Information

Chemical Name:ethyl styryldiazoacetate
CAS No.:126580-12-9
Molecular Formula:C₁₂H₁₂N₂O₂
Molecular Weight:216.239
Hs Code.:

Synonyms:ethyl styryldiazoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl styryldiazoacetate

Chemical Property:

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Technology Process of ethyl styryldiazoacetate

There total 6 articles about ethyl styryldiazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1205-84-1
ethyl (E)-4-phenylbut-3-enoate

: 126580-12-9
(E)-ethyl 2-diazo-4-phenylbut-3-enoate

Guidance literature:: With 4-acetylbenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at -20 - 20 ℃; for 0.5h;
DOI:10.1002/anie.201209301

Reference yield: 58.0%

: 126580-09-4
ethyl 2-diazo-3-hydroxy-4-phenylbutyrate

: 126580-12-9
(E)-ethyl 2-diazo-4-phenylbut-3-enoate

Guidance literature:: With pyridine; trichlorophosphate; 1) 0 deg C, 6 h, 2) r.t., 12 h;
DOI:10.1021/jo00300a035

Reference yield: 49.0%

: 623-73-4
diazoacetic acid ethyl ester

: 588-72-7,1340-14-3
[(E)-2-bromoethenyl]benzene

: 126580-12-9
(E)-ethyl 2-diazo-4-phenylbut-3-enoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; silver carbonate; In toluene; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja513275c