O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

Base Information

Chemical Name:O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester
CAS No.:1067639-83-1
Molecular Formula:C₂₁H₂₀N₂O₇
Molecular Weight:412.399
Hs Code.:

Synonyms:O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

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Chemical Property of O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

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Technology Process of O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

There total 1 articles about O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 868285-96-5
(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

: 524-38-9
N-hydroxyphthalimide

: 1067639-83-1
O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

Guidance literature:: N-hydroxyphthalimide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1055/s-2008-1078600

Reference yield: 53.0%

: 1067639-83-1
O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

: 152120-54-2,862686-58-6,1143572-00-2
N,N'-bis( tert-butoxycarbonyl)-1H-pyrazole-1-carboxamidine

: (S)-methyl 11-(((benzyloxy)carbonyl)amino)-6-((tert-butoxycarbonyl)amino)-2,2-dimethyl-4-oxo-3,8-dioxa-5,7-diazadodec-5-en-12-oate

Guidance literature:: O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester; With methylhydrazine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

N,N'-bis( tert-butoxycarbonyl)-1H-pyrazole-1-carboxamidine; With triethylamine; In tetrahydrofuran; Inert atmosphere;
DOI:10.1021/acsmedchemlett.5b00336