(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

Base Information

Chemical Name:(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate
CAS No.:868285-96-5
Molecular Formula:C₁₄H₁₉NO₇S
Molecular Weight:345.373
Hs Code.:

Synonyms:(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

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Technology Process of (S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

There total 1 articles about (S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: 314728-04-6
(S)-2-benzyloxycarbonylamino-4-hydroxybutyric acid methyl ester

: 868285-96-5
(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1055/s-2008-1078600

Reference yield: 88.0%

: 868285-96-5
(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

: (S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester

Guidance literature:: With sodium iodide; In acetone; for 0.666667h; Reflux;
DOI:10.1039/c6ob01187j

Reference yield: 71.0%

: 868285-96-5
(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate

: 524-38-9
N-hydroxyphthalimide

: 1067639-83-1
O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-N-[(phenylmethoxy)carbonyl]-L-homoserine methyl ester

Guidance literature:: N-hydroxyphthalimide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

(S )-methyl 2-(((benzyloxy)carbonyl)amino)-4-((methylsulfonyl)oxy)butanoate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1055/s-2008-1078600