Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

Base Information

Chemical Name:Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide
CAS No.:76248-61-8
Molecular Formula:C₁₈H₈F₁₂O₃P*K
Molecular Weight:570.313
Hs Code.:

Synonyms:Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

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Chemical Property of Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

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Technology Process of Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

There total 10 articles about Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 100-52-7
benzaldehyde

: 508230-18-0,191416-27-0
C₂₂H₁₅F₁₂O₄P

: 4610-69-9
(Z)-ethyl cinnamate

: 76248-61-8
Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

Guidance literature:: C₂₂H₁₅F₁₂O₄P; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

benzaldehyde; In tetrahydrofuran; at -20 ℃; for 3h;
DOI:10.1021/ja964122w

Reference yield: 77.0%

: 552-89-6
2-nitro-benzaldehyde

: 508230-18-0,191416-27-0
C₂₂H₁₅F₁₂O₄P

: 76248-61-8
Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

: 94527-24-9
3-(2-nitrophenyl)acrylic acid ethyl ester

Guidance literature:: C₂₂H₁₅F₁₂O₄P; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

2-nitro-benzaldehyde; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/ja964122w

Reference yield: 75.0%

: 630-19-3
pivalaldehyde

: C₂₇H₁₇F₁₂O₄P

: 76248-61-8
Potassium 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'-spiro<1H,3H,-2,1-benzoxaphosphole>-1-oxide

: (Z)-4,4-Dimethyl-pent-2-enoic acid benzyl ester

Guidance literature:: C₂₇H₁₇F₁₂O₄P; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

pivalaldehyde; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ja964122w