C₂₆H₂₈NOP

Base Information

Chemical Name:C₂₆H₂₈NOP
CAS No.:192372-08-0
Molecular Formula:C₂₆H₂₈NOP
Molecular Weight:401.488
Hs Code.:

Synonyms:C₂₆H₂₈NOP

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Chemical Property of C₂₆H₂₈NOP

Chemical Property:

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Technology Process of C₂₆H₂₈NOP

There total 6 articles about C₂₆H₂₈NOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 192371-97-4
C₂₆H₂₈NOPS

: 192372-08-0
C₂₆H₂₈NOP

Guidance literature:: With Raney nickel (Ra-Ni); In acetonitrile; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c1cc13785a

Reference yield:

: 354816-38-9
(S)-3-(diphenylphosphorothioyl)-3-phenylpropanoic acid

: 192372-08-0
C₂₆H₂₈NOP

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; acetonitrile / 6 h / 20 °C / Inert atmosphere

2: lithium borohydride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

3: methanesulfonyl chloride; triethylamine / dichloromethane / 20 °C / Inert atmosphere

4: Raney nickel (Ra-Ni) / acetonitrile / 48 h / 20 °C / Inert atmosphere

With lithium borohydride; benzotriazol-1-ol; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/c1cc13785a

Reference yield:

: 829-85-6
diphenylphosphane

: 192372-08-0
C₂₆H₂₈NOP

Guidance literature:: Multi-step reaction with 6 steps

1.1: (S,S)-((C₆H₃)(CH(CH₃)PPh₂)2)PdOAc) / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 2 h / Reflux

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; acetonitrile / 6 h / 20 °C / Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

5.1: methanesulfonyl chloride; triethylamine / dichloromethane / 20 °C / Inert atmosphere

6.1: Raney nickel (Ra-Ni) / acetonitrile / 48 h / 20 °C / Inert atmosphere

With lithium borohydride; (S,S)-((C₆H₃)(CH(CH₃)PPh₂)2)PdOAc); benzotriazol-1-ol; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c1cc13785a