3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Base Information

Chemical Name:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester
CAS No.:116527-86-7
Molecular Formula:C₃₄H₃₈N₂O₅
Molecular Weight:554.686
Hs Code.:

Synonyms:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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Chemical Property of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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Technology Process of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

There total 9 articles about 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 67-56-1
methanol

: 116527-83-4
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

: 116527-86-7
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: With Amberlyst 15; at 60 ℃; for 144h;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield: 68.0%

: 67-56-1
methanol

: 116527-81-2
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

: 116527-86-7
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: With hydrogenchloride; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116527-86-7
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

3: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; water; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)86862-9