2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

Base Information

Chemical Name:2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide
CAS No.:1092977-28-0
Molecular Formula:C₂₂H₃₆N₂O₄
Molecular Weight:392.539
Hs Code.:

Synonyms:2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

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Chemical Property of 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

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Technology Process of 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

There total 7 articles about 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1092977-08-6
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

: 74-88-4
methyl iodide

: 1092977-28-0
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

Guidance literature:: 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

methyl iodide; In tetrahydrofuran; for 2h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1092977-28-0
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide / acetic acid / 16 h / 0 - 80 °C

1.2: 16 h / 20 °C

2.1: potassium carbonate / acetone / 72 h / Heating / reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

3.2: 16 h / 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: 2 h / -78 - 20 °C

With hydrogen bromide; sodium hydride; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; acetone;

Reference yield:

: 29973-97-5
2-(3-benzyloxyphenyl)ethyl amine hydrochloride

: 1092977-28-0
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylpropanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 1810.07 Torr

3.1: potassium carbonate / acetone / 72 h / Heating / reflux

4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

4.2: 16 h / 20 °C

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

5.2: 2 h / -78 - 20 °C

With sodium hydroxide; hydrogen; sodium hydride; potassium carbonate; lithium hexamethyldisilazane; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;