allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside
CAS No.:1091625-60-3
Molecular Formula:C₅₈H₆₉NO₁₅
Molecular Weight:1020.18
Hs Code.:

Synonyms:allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

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Technology Process of allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

There total 4 articles about allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1061181-65-4
allyl (3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroacetamido)-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

: 108-24-7
acetic anhydride

: 1091625-60-3
allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: allyl (3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroacetamido)-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside; With methanol; sodium methylate; In dichloromethane; for 9h;

acetic anhydride; In methanol; dichloromethane; for 2h; Further stages.;
DOI:10.1016/j.tet.2008.08.080

Reference yield: 5.0%

: 67-56-1
methanol

: 1095608-62-0
C₆₄H₇₅NO₁₈

: 124-41-4
sodium methylate

: 108-24-7
acetic anhydride

: 1091625-60-3
allyl (2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

: 1091625-61-4
allyl (2-deoxy-2-methylcarbamate-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: methanol; C₆₄H₇₅NO₁₈; sodium methylate; In dichloromethane; for 9h;

acetic anhydride; In methanol; for 2h;
DOI:10.1021/jo802127z