2-CHLOROPHENOXYACETIC ACID HYDRAZIDE

Base Information

• Chemical Name: 2-CHLOROPHENOXYACETIC ACID HYDRAZIDE
• CAS No.: 36304-40-2
• Molecular Formula: C8H9ClN2O2
• Molecular Weight: 200.625
• Hs Code.: 2928000090
• Mol file: 36304-40-2.mol

Synonyms:Acetic acid, (o-chlorophenoxy)-,hydrazide (6CI);(2-Chlorophenoxyacetyl)hydrazide;(o-Chlorophenoxy)acetic acid hydrazide;2-(2-Chlorophenoxy)acetohydrazide;

Chemical Property of 2-CHLOROPHENOXYACETIC ACID HYDRAZIDE

Chemical Property:

• Vapor Pressure: 2.95E-07mmHg at 25°C
• Melting Point: 111-112 °C
• Refractive Index: 1.568
• Boiling Point: 419.8 °C at 760 mmHg
• Flash Point: 207.7 °C
• PSA: 64.35000
• Density: 1.324 g/cm³
• LogP: 1.79990
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-(2-Chlorophenoxy)acetohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLOROPHENOXYACETIC ACID HYDRAZIDE

There total 8 articles about 2-CHLOROPHENOXYACETIC ACID HYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-(2-chlorophenoxy)-N-(1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)acetamide → 2-amino-1H-benzo[de]isoquinoline-1,3(2H)-dione (5690-46-0) + (2-chlorophenoxy)acetic acid hydrazide (36304-40-2)

Guidance literature:

With hydrazine hydrate; In ethanol; for 3h; Reflux;

DOI:10.1002/chem.202102593

Reference yield: 68.0%

ethyl 2-(2-chlorophenoxy)acetate (52094-97-0) → (2-chlorophenoxy)acetic acid hydrazide (36304-40-2)

Guidance literature:

With hydrazine hydrate; In methanol; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2010.11.034

Reference yield:

(2-chlorophenoxy)acetic acid (614-61-9) → (2-chlorophenoxy)acetic acid hydrazide (36304-40-2)

Guidance literature:

With hydrazine hydrate; sulfuric acid; In methanol; for 25h; Heating;

DOI:10.1211/0022357011775307

upstream raw materials:

Methyl (2-chlorophenoxy)acetate

ethyl 2-(2-chlorophenoxy)acetate

(2-chlorophenoxy)acetic acid

2-monochlorophenol

Downstream raw materials:

(2-chloro-phenoxymethyl)-carbamic acid isopropyl ester

(2-chloro-phenoxymethyl)-carbamic acid-(2-chloro-ethyl ester)

5-(2-chloro-phenoxymethyl)-[1,3,4]oxadiazol-2-ylamine

(2-Chloro-phenoxy)-acetic acid [2-oxo-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide

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