5-Benzyloxyvaleric acid methyl ester

Base Information

Chemical Name:5-Benzyloxyvaleric acid methyl ester
CAS No.:31662-20-1
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:
Mol file:31662-20-1.mol

Synonyms:5-benzyloxypentanoic acid methyl ester

Suppliers and Price of 5-Benzyloxyvaleric acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Atlantic Research Chemicals
Methyl5-(Benzyloxy)pentanoate 95%
1gm:
$ 420.61

A1 Biochem Labs
Methyl5-(Benzyloxy)pentanoate 95%
1 g
$ 400.00

Total 3 raw suppliers

Chemical Property of 5-Benzyloxyvaleric acid methyl ester

Chemical Property:

Boiling Point:293.7±23.0 °C(Predicted)
Density:1.035±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Methyl5-(Benzyloxy)pentanoate 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Benzyloxyvaleric acid methyl ester

There total 10 articles about 5-Benzyloxyvaleric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-56-1
methanol

: 64740-39-2
5-benzyloxypentanoic acid

: 31662-20-1
5-benzyloxypentanoic acid methyl ester

Guidance literature:: With thionyl chloride; for 15h; Ambient temperature;
DOI:10.1021/jo00115a013

Reference yield: 66.0%

: 67-56-1
methanol

: (5-benzenesulfonyl-5-nitropentyloxymethyl)benzene

: 31662-20-1
5-benzyloxypentanoic acid methyl ester

Guidance literature:: methanol; (5-benzenesulfonyl-5-nitropentyloxymethyl)benzene; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.166667h;

With ozone; In dichloromethane; at -78 ℃; for 0.166667h;
DOI:10.1016/j.tet.2019.130883

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 31662-20-1
5-benzyloxypentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: L-proline; ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol / dimethyl sulfoxide / 4 h / 40 °C / Sonication

2.1: sodium cyanoborohydride / N,N-dimethyl-formamide / 90 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.17 h / 0 °C

3.2: 0.17 h / -78 °C

With ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; L-proline; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2019.130883