2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

Base Information

Chemical Name:2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol
CAS No.:222558-57-8
Molecular Formula:C₃₁H₃₀N₂O₂
Molecular Weight:462.591
Hs Code.:

Synonyms:2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

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Chemical Property of 2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

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Technology Process of 2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

There total 1 articles about 2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 117-99-7
2-Hydroxybenzophenone

: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

: 222558-57-8
2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

Guidance literature:: In methanol; for 5h; Reflux;
DOI:10.1080/00958972.2015.1073268

Reference yield: 94.1%

: 222558-57-8
2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

: 6046-93-1
copper(II) acetate monohydrate

: C₃₁H₂₈CuN₂O₂

Guidance literature:: In methanol; for 1h; Reflux;
DOI:10.1007/s10973-017-6563-2

Reference yield: 50.0%

: 31011-57-1,112925-19-6,112925-18-5
tetrachlorobis(tetrahydrofuran)titanium(IV)

: 222558-57-8
2,2'-((2,2-dimethylpropane-1,3-diyl)bis((nitrilo)(phenylmethylidyne)))diphenol

: 222558-48-7
OC₆H₄C(C₆H₅)NCH₂C(CH₃)2CH₂NC(C₆H₅)C₆H₄OTiCl₂

Guidance literature:: With NaH; In tetrahydrofuran; byproducts: H2, NaCl; addn. of NaH to ligand in THF, stirring till comnplete H2-evolution, refluxing (2 h), cooling to -78°C, slow addn. of Ti-complex, stirring (50°C, 5 h), filtration, extn. of residue (toluene), evapn. of filtrate, washing (toluene); IR, MS, NMR, elem. anal.;
DOI:10.1039/a808372j