2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

Base Information

Chemical Name:2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene
CAS No.:606965-20-2
Molecular Formula:C₂₀H₃₃N₃OSSe
Molecular Weight:442.528
Hs Code.:

Synonyms:2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

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Chemical Property of 2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

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Technology Process of 2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

There total 2 articles about 2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7433-56-9
(E)-5-decene

: 438497-46-2
C₁₁H₁₃F₃O₄S₂Se

: 2-((1R,2S)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

: 606965-20-2
2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

Guidance literature:: C₁₁H₁₃F₃O₄S₂Se; With sodium azide; In acetonitrile; at -30 ℃; for 0.5h;

(E)-5-decene; In acetonitrile; at -30 - 20 ℃; for 20h; Title compound not separated from byproducts;
DOI:10.1002/anie.200351229

Reference yield:

: 438497-31-5
di-[2-methoxy-6-[(1S)-1-(methylthio)ethyl]phenyl]diselenide

: 606965-20-2
2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Br₂ / acetonitrile / 0 °C

2.1: NaN₃ / acetonitrile / 0.5 h / -30 °C

2.2: acetonitrile / 20 h / -30 - 20 °C

With sodium azide; bromine; In acetonitrile;
DOI:10.1002/anie.200351229

Reference yield:

: 606965-20-2
2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene

: (1R,2S)-1-Butyl-2-[2-methoxy-6-((S)-1-methylsulfanyl-ethyl)-phenylselanyl]-hexylamine

Guidance literature:: 2-((1S,2R)-2-Azido-1-butyl-hexylselanyl)-1-methoxy-3-((S)-1-methylsulfanyl-ethyl)-benzene; With triphenylphosphine; In tetrahydrofuran;

With water; In tetrahydrofuran; at 50 ℃;
DOI:10.1002/anie.200351229