(1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2

Base Information

Chemical Name:(1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2
CAS No.:97295-81-3
Molecular Formula:C₂₈H₃₀O₂P₂Pt
Molecular Weight:655.573
Hs Code.:

Synonyms:(1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2

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Chemical Property of (1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2

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Technology Process of (1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2

There total 3 articles about (1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 83095-83-4,14647-25-7
[platinum(II)dichloride(1,2-bis(diphenylphosphino)ethane)]

: 124-41-4
sodium methylate

: 97295-81-3
(1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2

Guidance literature:: In methanol; benzene; slurry of (DPPE)PtCl2 in benzene treated with soln. of NaOCH3 in methanol and mixt. stirred at ambient temp. for 2 h; soln. concd., pentane added, solid filtered and dried in stream of nitrogen, solid extd. with THF, soln. concd., pentane added, solid collectedand vac. dried, solid recrystd. from CH2Cl2/pentane;
DOI:10.1021/ja00276a018

Reference yield:

: 67-56-1
methanol

: 438188-08-0
Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(OSi(CH₂CH₃)3)2

: 97295-81-3
(1,2-bis(diphenylphosphino)-ethane)Pt(OMe)2

Guidance literature:: In benzene-d6; byproducts: (CH3CH2)3SiOH; (N2); addn. of MeOH to a soln. of platinum complex in C6D6, stirring for4 h; detected by NMR;