sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

Base Information

Chemical Name:sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate
CAS No.:1207989-12-5
Molecular Formula:C₄₁H₄₄ClN₂O₅S*Na
Molecular Weight:735.32
Hs Code.:

Synonyms:sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

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Chemical Property of sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

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Technology Process of sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

There total 13 articles about sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-35-7
Tau

: 1207990-15-5
4-{2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl}benzoic acid

: 1207989-12-5
sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

Guidance literature:: Tau; 4-{2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl}benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

With hydrogenchloride; In water;

With sodium hydrogencarbonate; In methanol; water; acetonitrile;

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1207989-12-5
sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichlorobis(tri-O-tolylphosphine)palladium; sodium carbonate / ethanol; water; 1,2-dimethoxyethane / 2 h / 125 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 1 h / 20 °C

2.2: 1.5 h / Reflux

3.1: hydrogenchloride / water; 1,4-dioxane / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

With hydrogenchloride; oxalyl dichloride; dichlorobis(tri-O-tolylphosphine)palladium; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1207989-56-7
[4-((R)-4-tert-butylcyclohex-1-enyl)phenyl]acetic acid ethyl ester

: 1207989-12-5
sodium 2-{4-[2-[4-(4-(R)-tert-butylcyclohex-1-enyl)phenyl]-2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)ethyl]benzoylamino}ethanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.1: lithium hydroxide; water / tetrahydrofuran; methanol / 5 h / 20 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 1 h / 20 °C

3.2: 1.5 h / Reflux

4.1: hydrogenchloride / water; 1,4-dioxane / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

With hydrogenchloride; oxalyl dichloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;