Technology Process of C56H58N2O18
There total 8 articles about C56H58N2O18 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C64H74N2O18;
With
sodium hydroxide;
In
methanol;
at 55 ℃;
With
hydrogenchloride;
In
water;
at 20 ℃;
DOI:10.1021/ja410443n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetonitrile / Inert atmosphere; Reflux
2.1: triethylamine / dichloromethane / 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
4.1: sodium hydroxide / methanol / 55 °C
4.2: 20 °C
With
potassium carbonate; triethylamine; sodium hydroxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja410443n
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: zinc; titanium tetrachloride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere
2.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere
3.1: potassium carbonate / acetonitrile / Inert atmosphere; Reflux
4.1: triethylamine / dichloromethane / 20 °C
5.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
6.1: sodium hydroxide / methanol / 55 °C
6.2: 20 °C
With
boron tribromide; titanium tetrachloride; potassium carbonate; triethylamine; sodium hydroxide; zinc;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja410443n
