2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

Base Information

Chemical Name:2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester
CAS No.:457060-10-5
Molecular Formula:C₂₁H₂₄O₆
Molecular Weight:372.418
Hs Code.:

Synonyms:2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

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Chemical Property of 2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

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Technology Process of 2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

There total 1 articles about 2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 93-15-2
1,2-dimethoxy-4-(2-propenyl)benzene

: 17667-32-2
methyl 6-bromo-3,4-dimethoxybenzoate

: 457060-10-5
2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; for 24h; Heating;
DOI:10.1021/ol026074s

Reference yield: 76.0%

: 457060-10-5
2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

: 65047-63-4
2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthol

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h;
DOI:10.1021/ol026074s

Reference yield:

: 457060-10-5
2-[(E)-3-(3,4-Dimethoxy-phenyl)-propenyl]-4,5-dimethoxy-benzoic acid methyl ester

: 322765-98-0
permethyl ningalin C

Guidance literature:: Multi-step reaction with 4 steps

1.1: 76 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 3 h / -78 - 20 °C

2.1: 62 percent / hydrogen peroxide; iodine; sulfuric acid / methanol / 4 h / 20 °C

3.1: 80 percent / ethanol / 24 h / 20 °C

4.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / -78 °C

4.2: 73 percent / lithium diisopropylamide / tetrahydrofuran; hexane / -78 - 20 °C

With sulfuric acid; dihydrogen peroxide; iodine; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; hexane;
DOI:10.1021/ol026074s