methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

Base Information

Chemical Name:methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate
CAS No.:1615740-30-1
Molecular Formula:C₁₉H₂₉ClN₂O₃
Molecular Weight:368.904
Hs Code.:

Synonyms:methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

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Chemical Property of methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

Chemical Property:

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Technology Process of methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

There total 5 articles about methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: methyl 5-chloro-3-(ethyl(piperidin-4-yl)amino)-2-methylbenzoate

: 6482-24-2
2-Bromoethyl methyl ether

: 1615740-30-1
methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 60 ℃; for 16h;

Reference yield:

: 1403595-31-2
tert-butyl 4-((5-chloro-3-(methoxycarbonyl)-2-methylphenyl)-amino)-piperidine-1-carboxylate

: 1615740-30-1
methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C

1.2: 12 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

3.1: potassium carbonate; potassium iodide / acetonitrile / 16 h / 60 °C

With potassium carbonate; acetic acid; trifluoroacetic acid; potassium iodide; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 294190-18-4
methyl 3-amino-5-chloro-2-methylbenzoate

: 1615740-30-1
methyl 5-chloro-3-(ethyl(1-(2-methoxyethyl)piperidin-4-yl)amino)-2-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C

1.2: 16 h / 0 - 20 °C

2.1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C

2.2: 12 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

4.1: potassium carbonate; potassium iodide / acetonitrile / 16 h / 60 °C

With potassium carbonate; acetic acid; trifluoroacetic acid; potassium iodide; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;