N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

Base Information

Chemical Name:N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester
CAS No.:247223-85-4
Molecular Formula:C₂₄H₂₄N₂O₄
Molecular Weight:404.466
Hs Code.:

Synonyms:N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

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Chemical Property of N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

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Technology Process of N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

There total 8 articles about N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 247223-83-2
N-(2-(β-Aminoethyl)phenyl)anthranilsaeuremethylester

: 247223-85-4
N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 60h;

Reference yield:

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 247223-85-4
N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

Guidance literature:: Multi-step reaction with 7 steps

1: 68 percent / K₂CO₃ / Cu; CuI / dibutyl ether / 22 h / 175 °C

2: 99 percent / aq. HCl / acetone / 1.5 h / 30 °C

3: 99 percent / NaBH₄ / diethyl ether / Heating

4: SOCl₂; pyridine / diethyl ether / 1 h

5: dimethylsulfoxide / 1 h / 40 °C

6: 84 percent / BH₃*THF / tetrahydrofuran / 1.5 h / Heating

7: 70 percent / K₂CO₃ / CH₂Cl₂ / 60 h / 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; thionyl chloride; borane-THF; potassium carbonate; copper(l) iodide; copper; In tetrahydrofuran; diethyl ether; dichloromethane; dibutyl ether; dimethyl sulfoxide; acetone; 1: Substitution / 2: Ring cleavage / 3: Reduction / 4: Chlorination / 5: Substitution / 6: Reduction / 7: Carboxylation;

Reference yield:

: 134-20-3
2-carbomethoxyaniline

: 247223-85-4
N-(2-(β-(N'-Benzyloxycarbonyl)aminoethyl)phenyl)anthranilsaeuremethylester

Guidance literature:: Multi-step reaction with 7 steps

1: 68 percent / K₂CO₃ / Cu; CuI / dibutyl ether / 22 h / 175 °C

2: 99 percent / aq. HCl / acetone / 1.5 h / 30 °C

3: 99 percent / NaBH₄ / diethyl ether / Heating

4: SOCl₂; pyridine / diethyl ether / 1 h

5: dimethylsulfoxide / 1 h / 40 °C

6: 84 percent / BH₃*THF / tetrahydrofuran / 1.5 h / Heating

7: 70 percent / K₂CO₃ / CH₂Cl₂ / 60 h / 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; thionyl chloride; borane-THF; potassium carbonate; copper(l) iodide; copper; In tetrahydrofuran; diethyl ether; dichloromethane; dibutyl ether; dimethyl sulfoxide; acetone; 1: Substitution / 2: Ring cleavage / 3: Reduction / 4: Chlorination / 5: Substitution / 6: Reduction / 7: Carboxylation;