1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

Base Information

Chemical Name:1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide
CAS No.:1489288-61-0
Molecular Formula:C₂₃H₂₂ClN₃O₂S
Molecular Weight:439.966
Hs Code.:

Synonyms:1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

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Chemical Property of 1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

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Technology Process of 1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

There total 3 articles about 1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31162-25-1
1-(isothiocyanatomethyl)-4-phenylbenzene

: 1489290-58-5
C₉H₁₁ClN₂O₂

: 1489288-61-0
1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

Guidance literature:: In N,N-dimethyl-formamide; at 55 ℃; for 1.5h;
DOI:10.1016/j.ejmech.2013.08.027

Reference yield:

: 4122-68-3
4-chlorophenyloxyacetyl chloride

: 1489288-61-0
1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 1.5 h / 55 °C

In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.08.027

Reference yield:

: 712-76-5
N-(4-phenyl)benzylamine

: 1489288-61-0
1-(4-chlorophenoxyacetyl)-1-methyl-4-(4-phenylbenzyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 1.5 h / 55 °C / Molecular sieve

2: N,N-dimethyl-formamide / 1.5 h / 55 °C

In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.08.027