2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide

Base Information

• Chemical Name: 2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide
• CAS No.: 83026-54-4
• Molecular Formula: C₁₅H₂₅NO₂
• Molecular Weight: 251.369

Synonyms:2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide

Chemical Property of 2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide

Chemical Property:

Purity/Quality:

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Technology Process of 2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide

There total 2 articles about 2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

tert.-butylhydroperoxide (75-91-2) + 2-<4-(dimethylamino)phenyl>-2-propanol (83026-55-5) → 2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide (83026-54-4)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; for 2.5h; Ambient temperature;

DOI:10.1021/jo00144a022

Reference yield:

ethyl p-dimethyaminolbenzoate (10287-53-3) → 2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide (83026-54-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent

2: 28 percent / p-toluenesulfonic acid / CH₂Cl₂ / 2.5 h / Ambient temperature

With toluene-4-sulfonic acid; In dichloromethane;

DOI:10.1021/jo00144a022

Reference yield: 21.0%

2-<4-(dimethylamino)phenyl>propyl tert-butyl peroxide (83026-54-4) → 2-<4-(dimethylamino)phenyl>-2-propanol (83026-55-5) + acetone (67-64-1) + tert-butyl alcohol (75-65-0)

Guidance literature:

In chlorobenzene; at 129.2 ℃; Product distribution; Rate constant; with styrene addition;

DOI:10.1021/jo00144a022

upstream raw materials:

tert.-butylhydroperoxide

2-<4-(dimethylamino)phenyl>-2-propanol

ethyl p-dimethyaminolbenzoate

Downstream raw materials:

2-<4-(dimethylamino)phenyl>-2-propanol

acetone

tert-butyl alcohol

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