(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

Base Information

Chemical Name:(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid
CAS No.:1235458-26-0
Molecular Formula:C₂₇H₂₂Cl₂N₂O₆S
Molecular Weight:573.453
Hs Code.:

Synonyms:(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

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Chemical Property of (Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

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Technology Process of (Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

There total 1 articles about (Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 477573-39-0
5-[(2,6-dichlorobenzyl)sulfonyl]-1,3-dihydro-2H-indol-2-one

: C₁₂H₁₃NO₄

: 1235458-26-0
(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

Guidance literature:: With piperidine; In ethanol; for 12h; Reflux;
DOI:10.1039/c4ra08720h

Reference yield: 92.0%

: 64-17-5
ethanol

: 1235458-26-0
(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

: 1235459-42-3
(Z)-ethyl-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoate

Guidance literature:: With thionyl chloride; for 12h; Reflux;
DOI:10.1039/c4ra08720h

Reference yield: 85.0%

: 1235458-26-0
(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid

: 74-89-5
methylamine

: 1235459-01-4
(Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)-N-methylpropanamide

Guidance literature:: (Z)-3-(2-{[5-(2,6-dichlorobenzylsulfonyl)-2-oxoindolin-3-ylidene]-methyl}-4-oxo-4,5,6,7-tetrahydro-1H-indol-3-yl)propanoic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 3h;

methylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/c4ra08720h