N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

Base Information

Chemical Name:N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide
CAS No.:887250-03-5
Molecular Formula:C₁₆H₂₂N₂OS
Molecular Weight:290.429
Hs Code.:

Synonyms:N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

There total 5 articles about N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: (S)-4-methyl-N-[(1E)-(trans-4-methylcyclohexyl)methylidene]benzene-1-sulfinamide

: 5804-85-3
diethylaluminium cyanide

: 887250-03-5
N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

Guidance literature:: diethylaluminium cyanide; In tetrahydrofuran; isopropyl alcohol; toluene; at -78 ℃;

(S)-4-methyl-N-[(1E)-(trans-4-methylcyclohexyl)methylidene]benzene-1-sulfinamide; In tetrahydrofuran; isopropyl alcohol; toluene; at -78 - 20 ℃;

Reference yield:

: 3937-49-3
(trans-4-methylcyclohexyl)methanol

: 887250-03-5
N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 16 h / -10 - 20 °C

2.1: titanium(IV) tetraethanolate / dichloromethane / 2 h / Reflux

3.1: tetrahydrofuran; toluene; isopropyl alcohol / -78 °C

3.2: -78 - 20 °C

With titanium(IV) tetraethanolate; sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; isopropyl alcohol; toluene;

Reference yield:

: 7133-05-3
trans-4-(methyl)cyclohexane-1-carbaldehyde

: 887250-03-5
N-[(S)-cyano(trans-4-methylcyclohexyl)methyl]-(S)-4-methylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / dichloromethane / 2 h / Reflux

2.1: tetrahydrofuran; toluene; isopropyl alcohol / -78 °C

2.2: -78 - 20 °C

With titanium(IV) tetraethanolate; In tetrahydrofuran; dichloromethane; isopropyl alcohol; toluene;