α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

Base Information

Chemical Name:α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride
CAS No.:82933-38-8
Molecular Formula:C₁₂H₁₆N₂O₅*ClH
Molecular Weight:304.73
Hs Code.:

Synonyms:α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

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Chemical Property of α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

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Technology Process of α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

There total 1 articles about α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 28832-02-2
benzyl [(4R)-3-oxo-1,2-oxazolidin-4-yl]carbamate

: 82933-38-8
α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; acetyl chloride; Yield given. Multistep reaction; 1.) 0-5 deg C, 30 min, 2.) 0-26 deg C, 12 h;
DOI:10.1021/ja00386a035

Reference yield: 81.9%

: 1145-80-8
N-(benzyloxycarbonyl)-L-serine

: 82933-38-8
α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

: 82933-39-9
(R)-2-Benzyloxycarbonylamino-3-((S)-2-benzyloxycarbonylamino-3-hydroxy-propionylaminooxy)-propionic acid methyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In water; for 0.333333h; pH 4.2;
DOI:10.1021/ja00386a035

Reference yield:

: 82933-38-8
α-((benzyloxy)carbonyl)-β-aminoxy-D-alanine methyl ester hydrochloride

: (R)-2-Benzyloxycarbonylamino-3-((S)-3-benzyloxycarbonylamino-2-oxo-azetidin-1-yloxy)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81.9 percent / 1-ethyl-3-(3-(dimethylamino)propyl)carbodiimide / H₂O / 0.33 h / pH 4.2

2: diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 12 h / 0 - 5 °C

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water;
DOI:10.1021/ja00386a035