N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide
• CAS No.: 135822-89-8
• Molecular Formula: C₁₅H₁₃NO₄S
• Molecular Weight: 303.339

Synonyms:N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide

Chemical Property of N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide

There total 7 articles about N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-[benzo[1,3]dioxol-5-yl-(toluene-4-sulfonyl)-methyl]-4-methyl-benzenesulfonamide → (E)-N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methylbenzenesulfonamide (135822-89-8)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1080/00397910601131387

Reference yield: 93.0%

piperonal (120-57-0,30024-74-9) + toluene-4-sulfonamide (70-55-3) → N-[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-4-methyl-benzenesulfonamide (135822-89-8)

Guidance literature:

With peroxodisulfate ion; zirconium(IV) oxide; for 0.0333333h; microwave irradiation;

DOI:10.1081/SCC-120030315

Reference yield: 92.0%

piperonal (120-57-0,30024-74-9) + toluene-4-sulfonamide (70-55-3) → (E)-N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methylbenzenesulfonamide (135822-89-8)

Guidance literature:

Sulfate; titanium(IV) oxide; In toluene; for 0.416667h; Heating;

upstream raw materials:

4-toluenesulfonyl azide

piperonal

chloroamine-T

toluene-4-sulfonamide

Downstream raw materials:

C₂₇H₂₉NO₈S

(S)-3-[(S)-1-(p-methylbenzenesulfonylamino)-1-(benzo[d][1,3]dioxol-5-yl)methyl]-3-methylindolin-2-one

N-(benzo[d][1,3]dioxol-5-yl(phenyl)methyl)-4-methylbenzenesulfonamide

(2S,3S)-methyl 3-(benzo[d][1,3]dioxol-5-yl)-2-(diphenylmethyleneamino)-3-(4-methylphenylsulfonamido)propanoate

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