4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

Base Information

Chemical Name:4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide
CAS No.:1015414-34-2
Molecular Formula:C₂₆H₂₈N₄OS₂
Molecular Weight:476.667
Hs Code.:

Synonyms:4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

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Chemical Property of 4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

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Technology Process of 4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

There total 4 articles about 4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1003639-38-0
4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]piperidine

: 19241-15-7
2,5-dimethylphenyl isothiocyanate

: 1015414-34-2
4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

Guidance literature:: In dichloromethane; at 20 ℃; for 0.35h;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1015414-34-2
4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine / ethanol; water / 1 h / 60 °C

1.2: 3 h / 20 °C

2.1: hydrogenchloride / dichloromethane; diethyl ether / 1 h / 20 °C

3.1: dichloromethane; acetic acid methyl ester / 0 - 20 °C

With hydrogenchloride; hydroxylamine; In diethyl ether; ethanol; dichloromethane; acetic acid methyl ester; water;

Reference yield:

: 869901-02-0
tert-butyl 4-(4-formyl-1,3-thiazol-2-yl)tetrahydro-1(2H)-pyridinecarboxylate

: 1015414-34-2
4-[4-(4,5-dihydro-5-phenyl-3-isoxazolyl)-2-thiazolyl]-N-(2,5-dimethylphenyl)-1-piperidinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine / ethanol; water / 1 h / 60 °C

1.2: 3 h / 20 °C

2.1: hydrogenchloride / dichloromethane; diethyl ether / 1 h / 20 °C

3.1: dichloromethane; acetic acid methyl ester / 0 - 20 °C

With hydrogenchloride; hydroxylamine; In diethyl ether; ethanol; dichloromethane; acetic acid methyl ester; water;