4,4'-Dimethylbenzophenone dimethyl acetal

Base Information

• Chemical Name: 4,4'-Dimethylbenzophenone dimethyl acetal
• CAS No.: 86456-47-5
• Molecular Formula: C₁₇H₂₀O₂
• Molecular Weight: 256.345
• Mol file: 86456-47-5.mol

Synonyms:4,4'-Dimethylbenzophenone dimethyl acetal

Chemical Property of 4,4'-Dimethylbenzophenone dimethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4'-Dimethylbenzophenone dimethyl acetal

There total 4 articles about 4,4'-Dimethylbenzophenone dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

methanol (67-56-1) + bis(4-methylphenyl)methanone hydrazone (55816-25-6) → 4,4'-Dimethylbenzophenone dimethyl acetal (86456-47-5) + 4,4'-dimethyldiphenylmethane (4957-14-6) + methyl bis(4-methylphenyl)methyl ether (18939-92-9)

Guidance literature:

With sodium methylate; at 70 ℃; C-anode, Pt-cathode, 5.4 F/mol, constant current 0.2 A, undivided cell;

DOI:10.1021/jo00166a006

Reference yield:

methanol (67-56-1) + 4,4'-dimethyl-benzophenone 4-phenyl-semicarbazone (21367-48-6) → bis(p-methylphenyl)-methanone (611-97-2) + 4,4'-Dimethylbenzophenone dimethyl acetal (86456-47-5) + N-phenyl methyl carbamate (2603-10-3)

Guidance literature:

With sodium methylate; potassium iodide; In tert-butyl alcohol; at 20 ℃; Electrochemical reaction;

DOI:10.1080/00397911.2012.667184

Reference yield:

bis(4-methylphenyl)methanone hydrazone (55816-25-6) → 4,4'-Dimethylbenzophenone dimethyl acetal (86456-47-5) + 4,4'-dimethyldiphenylmethane (4957-14-6) + methyl bis(4-methylphenyl)methyl ether (18939-92-9)

Guidance literature:

With sodium methylate; In methanol; at 70 ℃; C-anode, C-cathode, 4.5 F/mol, constant current 0.5 A, undivided cell;

DOI:10.1021/jo00166a006

upstream raw materials:

methanol

bis(4-methylphenyl)methanone hydrazone

4,4'-dimethyl-benzophenone 4-phenyl-semicarbazone