2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide

Base Information

Chemical Name:2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide
CAS No.:109803-53-4
Molecular Formula:C₁₃H₁₅Cl₂NO₂
Molecular Weight:288.174
Hs Code.:
DSSTox Substance ID:DTXSID801252317

Synonyms:2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide;DTXSID801252317;109803-53-4

Suppliers and Price of 2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:287.0479841
Heavy Atom Count:18
Complexity:295

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)C(=O)NC2CCCC2)Cl)Cl

Technology Process of 2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide

There total 4 articles about 2,3-Dichloro-N-cyclopentyl-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 109803-53-4
N-cyclopentyl-2,3-dichloro-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / Fe, Br₂ / 4 h / 90 °C

2: 1.) Mg, I₂ / 1.) THF, reflux, 2.) THF

3: SOCl₂, DMF / ethyl acetate / 10 h / Heating

4: Et₃N / ethyl acetate / Ambient temperature

With thionyl chloride; bromine; iodine; iron; magnesium; triethylamine; N,N-dimethyl-formamide; In ethyl acetate;
DOI:10.1021/jm00393a020

Reference yield:

: 55901-80-9
2,3-dichloro-4-methoxy-benzoic acid

: 109803-53-4
N-cyclopentyl-2,3-dichloro-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / ethyl acetate / 10 h / Heating

2: Et₃N / ethyl acetate / Ambient temperature

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In ethyl acetate;
DOI:10.1021/jm00393a020

Reference yield:

: 109803-52-3
1-bromo-2,3-dichloro-4-methoxybenzene

: 109803-53-4
N-cyclopentyl-2,3-dichloro-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, I₂ / 1.) THF, reflux, 2.) THF

2: SOCl₂, DMF / ethyl acetate / 10 h / Heating

3: Et₃N / ethyl acetate / Ambient temperature

With thionyl chloride; iodine; magnesium; triethylamine; N,N-dimethyl-formamide; In ethyl acetate;
DOI:10.1021/jm00393a020