(R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

Base Information

Chemical Name:(R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester
CAS No.:77971-35-8
Molecular Formula:C₁₇H₂₂NO₂PS
Molecular Weight:335.407
Hs Code.:

Synonyms:(R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

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Chemical Property of (R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

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Technology Process of (R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

There total 5 articles about (R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 77971-34-7
(2S,4S,5S)-2,5-diphenyl-3,4-dimethyl-1,3,2-thiazaphospholidin-2-one

: 77971-35-8
(R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

Guidance literature:: With hydrogenchloride; methanolate;
DOI:10.1016/S0040-4039(00)71165-8

Reference yield:

: 90-81-3,90-82-4,299-42-3,321-97-1,321-98-2,4125-58-0,34783-90-9,38732-95-5,53214-57-6,7009-81-6,90-83-5,6912-63-6
(S,S)-(+)-pseudoephedrine

: 77971-35-8
(R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine

2: 85 percent / t-butyl-magnesiumbromide / benzene / Heating

3: 100 percent / HCl or CH₃O^(1-)

With hydrogenchloride; methanolate; tert-butylmagnesium bromide; triethylamine; In benzene;
DOI:10.1016/S0040-4039(00)71165-8

Reference yield:

: 77971-33-6
2-phenyl-1,3,2-oxazaphospholidine-2-thione

: 77971-35-8
(R)-Phenyl-phosphonothioic acid O-methyl ester S-((1S,2S)-2-methylamino-1-phenyl-propyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / t-butyl-magnesiumbromide / benzene / Heating

2: 100 percent / HCl or CH₃O^(1-)

With hydrogenchloride; methanolate; tert-butylmagnesium bromide; In benzene;
DOI:10.1016/S0040-4039(00)71165-8