lychnopholide

Base Information

• Chemical Name: lychnopholide
• CAS No.: 77448-64-7
• Molecular Formula: C₂₀H₂₂O₆
• Molecular Weight: 358.391
• Mol file: 77448-64-7.mol

Synonyms:lychnopholide;(Z)-2-Methyl-2-butenoic acid (3aR,4S,6R,10Z,11aR)-2,3,3a,4,5,6,7,11a-octahydro-6,10-dimethyl-3-methylene-2,7-dioxo-6,9-epoxycyclodeca[b]furan-4-yl ester;

Chemical Property of lychnopholide

Chemical Property:

• Vapor Pressure: 6.82E-13mmHg at 25°C
• Boiling Point: 567.4°C at 760 mmHg
• Flash Point: 249.5°C
• PSA: 78.90000
• Density: 1.24g/cm³
• LogP: 2.55410

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of lychnopholide

There total 5 articles about lychnopholide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H18O5 → lychnopholide (77448-64-7)

Guidance literature:

Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane

2: dmap; triethylamine / tetrahydrofuran

With dmap; manganese(IV) oxide; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/acscentsci.1c00056

Reference yield:

C15H18O5 → atripliciolide tiglate (77448-64-7)

Guidance literature:

Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane

2: dmap; triethylamine / tetrahydrofuran

With dmap; manganese(IV) oxide; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/acscentsci.1c00056

Reference yield:

(E)-2-methyl-2-butenoic anhydride (14316-68-8) + atripliciolide (67815-63-8) → atripliciolide tiglate (77448-64-7)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran;

DOI:10.1021/acscentsci.1c00056

upstream raw materials:

(Z)-2-methyl-2-butenoic anhydride

atripliciolide

(E)-2-methyl-2-butenoic anhydride