Methanone, (3,4-dihydro-2H-1-benzopyran-6-yl)phenyl-

Base Information

Chemical Name:Methanone, (3,4-dihydro-2H-1-benzopyran-6-yl)phenyl-
CAS No.:101019-00-5
Molecular Formula:C16H14 O2
Molecular Weight:238.2812
Hs Code.:
DSSTox Substance ID:DTXSID60143669
Wikidata:Q83007651

Synonyms:6-Chromanyl phenyl ketone;Chroman, 6-benzoyl-;Ketone, 6-chromanyl phenyl;BRN 0207728;Methanone, (3,4-dihydro-2H-1-benzopyran-6-yl)phenyl-;2H-1-Benzopyran, 3,4-dihydro-6-benzyl-;NIOSH/OB1748000;(3,4-Dihydro-2H-1-benzopyran-6-yl)phenylmethanone;OB17480000;101019-00-5;4-17-00-05365 (Beilstein Handbook Reference);DTXSID60143669;LS-87119;LS-91213

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, (3,4-dihydro-2H-1-benzopyran-6-yl)phenyl-

Chemical Property:

Vapor Pressure:7.69E-07mmHg at 25°C
Boiling Point:407.2°C at 760 mmHg
Flash Point:189.6°C
Density:1.159g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:238.099379685
Heavy Atom Count:18
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C=CC(=C2)C(=O)C3=CC=CC=C3)OC1

Technology Process of Methanone, (3,4-dihydro-2H-1-benzopyran-6-yl)phenyl-

There total 9 articles about Methanone, (3,4-dihydro-2H-1-benzopyran-6-yl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 201230-82-2
carbon monoxide

: chroman-6-yl(phenyl)iodonium triflate

: 98-80-6
phenylboronic acid

: 101019-00-5
chroman-6-yl-phenyl ketone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; at 20 ℃; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/adsc.202100809

Reference yield:

: 493-08-3
chromane

: 98-88-4
benzoyl chloride

: 101019-00-5
chroman-6-yl-phenyl ketone

Guidance literature:: With carbon disulfide; aluminium trichloride;

Reference yield:

: 1,1'-(phenyl-λ³-iodanediyl)bis(4-(trifluoromethyl)pyridinium)trifluoromethanesulfonate

: 101019-00-5
chroman-6-yl-phenyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 0.67 h / 0 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / 20 °C / 760.05 Torr / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane;
DOI:10.1002/adsc.202100809